Analyses of the chemical structures of melanoidins by 13C NMR, 13C and 15N CP-MAS NMR spectrometry.

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Analyses of the Chemical Structures of Melanoidins by i 3 C and i 5 N CP - MAS NMR Spectrometry " i 3 c NMR , Fumitaka HAyAsE , Seon

alkyl methyl (IV), saturated, unsaturated or aromatic and carbonyl (V) carbons. The signals of IV and V disappeared on ozone-treatrnent. Studies using glycine-2-i3C revealed that most of the glycine is incorporated into the melanoidins, On iSN CP-MAS NMR, weak broad signals in the region of ON70ppm and strong signals in the region of 70-.120ppm with a shoulder at 120 -・ 170 ppm (VI) were observ...

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13C CP/MAS NMR studies of vitamin E model compounds.

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SYNTHESIS OF SOME SUBSTITUTED NAPHTHALENES VIA BENZYNE AND THEIR 13C-NMR AND 'H-NMR STUDIES

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Condensed Tannin Reactivity Inhibition by Internal Rearrangements: Detection by Cp-mas 13c Nmr

Tannin extracts were prepared from barks of maritime pine (Pinus maritimus), aleppo pine (Pinus halepensis), Norway spruce (Picea abies) and from a mixture of barks of different pine species (Pinus spp., namely 20% black pine (Pinus thunbergii)+ 30% Scots pine (Pinus sylvestris) + 20% maritime pine (Pinus maritimus) + 10% Aleppo Pine (Pinus halepensis) + 5% Douglas fir (Pseudotsuga menziesii) +...

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Glycerin-Induced Conformational Changes in Bombyx mori Silk Fibroin Film Monitored by 13C CP/MAS NMR and 1H DQMAS NMR

In order to improve the stiff and brittle characteristics of pure Bombyx mori (B. mori) silk fibroin (SF) film in the dry state, glycerin (Glyc) has been used as a plasticizer. However, there have been very limited studies on the structural characterization of the Glyc-blended SF film. In this study, (13)C Cross Polarization/Magic Angle Spinning nuclear magnetic resonance (CP/MAS NMR) was used ...

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ژورنال

عنوان ژورنال: Agricultural and Biological Chemistry

سال: 1986

ISSN: 0002-1369,1881-1280

DOI: 10.1271/bbb1961.50.1951